Chemistry 0620 · IGCSE · Experimental design

Experimental design — practice question

A student carries out an investigation into the temperature change when a 5 cm length of coiled magnesium ribbon reacts with excess dilute sulfuric acid. The student performs five experiments. Experiment 1 • Rinse a burette first with distilled water and then with dilute sulfuric acid. • Fill the burette with dilute sulfuric acid. Let some dilute sulfuric acid run out until the level is at the 0.0 cm^{3} mark. • Use the burette to transfer 30.0 cm^{3} of dilute sulfuric acid into a boiling tube. • Measure the starting temperature of the acid with a thermometer. • Write down the starting temperature. • Drop a coil of magnesium ribbon into the boiling tube. At the same moment, start a stop-watch. • Stir the contents of the boiling tube continuously using the thermometer. • After 1 minute, measure the temperature of the mixture in the boiling tube. • Write down this temperature. Experiment 2 • Refill the burette with dilute sulfuric acid. Let some dilute sulfuric acid run out until the level is at the 0.0 cm^{3} mark. • Use the burette to transfer 25.0 cm^{3} of dilute sulfuric acid into a fresh boiling tube. • Measure the starting temperature of the acid with the thermometer. • Write down the starting temperature. • Drop a coil of magnesium ribbon into the boiling tube. At the same moment, start the stop-watch. • Stir the contents of the boiling tube continuously using the thermometer. • After 1 minute, measure the temperature of the mixture in the boiling tube. • Write down this temperature. Experiment 3 • Repeat Experiment 2, but use 20.0 cm^{3} of dilute sulfuric acid instead of 25.0 cm^{3}. Experiment 4 • Repeat Experiment 2, but use 15.0 cm^{3} of dilute sulfuric acid instead of 25.0 cm^{3}. Experiment 5 • Repeat Experiment 2, but use 10.0 cm^{3} of dilute sulfuric acid instead of 25.0 cm^{3}.
(a)[4]

Complete Table 2.1 using the thermometer diagrams.

(b)[4]

Use Fig. 2.1 to complete a suitable y-axis scale and plot the results from Experiments 1 to 5. Then draw a line of best fit.

(c)[2]

Explain why the temperature increase varies as the volume of dilute sulfuric acid changes.

(d)[3]

Extend the line of best fit on your graph in Fig. 2.1 to work out the temperature increase if 33.0 cm^{3} of dilute sulfuric acid is used. Make it clear on Fig. 2.1 how you found your answer. temperature increase = ________

(e)[1]

On Fig. 2.1, sketch a line to represent the results you would expect. Label this line E.

(f(i))[1]

Give one reason why a burette, instead of a measuring cylinder, is used to measure the volume of the dilute sulfuric acid.

(f(ii))[1]

Explain why the contents of the boiling tube are stirred during each experiment.

(g)[2]

Describe one change to the apparatus that will give more accurate results. Explain your answer. change to apparatus ________ explanation ________

Worked solution & mark scheme

This 18-mark question has a full step-by-step worked solution and mark scheme. One marking point: M1 all initial temperatures correct (21.0, 21.5, 21.5, 22.0, 22.0)

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