Chemistry 9701 · AS & A Level · Nitrogen compounds

Nitrogen compounds — practice question

Serotonin may be made from the amino acid tryptophan in two stages.
(a(i))[2]

A tryptophan sample in a buffer of $\text{pH }5.9$ remains stationary during electrophoresis. Draw the ions produced by tryptophan at $\text{pH }1.0$ and at $\text{pH }5.9$.

(a(ii))[2]

Tryptophan can react with valine to make a dipeptide. Use the Data Booklet to sketch this dipeptide.

(b)[8]

Complete the table to show the product structures and the reaction type for each separate reaction between serotonin and the four reagents: Na, excess $\text{Br}_2\text{(aq)}$, excess $\text{CH}_3\text{COCl}$, and excess $\text{H}_2$/Pt catalyst.

(c)

Serotonin is changed by enzymes in the liver into compound $M$.

(c(i))[1]

Using the Data Booklet, suggest a way in which the infra-red spectrum of $M$ would be different from that of serotonin.

(c(ii))[2]

The proton NMR spectrum of $M$ dissolved in $\text{CDCl}_3$ contains eight peaks because the molecule has eight different kinds of proton. The proton NMR spectrum of $M$ dissolved in $\text{D}_2\text{O}$ was then measured. Predict how many peaks would appear in the proton NMR spectrum of $M$ in $\text{D}_2\text{O}$. Explain your answer.

(d)[1]

Compound $M$ can undergo polymerisation under suitable conditions to give polymer $N$, as shown. Polymer $N$ is biodegradable, whereas polyethene is not. Explain why $N$ is biodegradable.

Worked solution & mark scheme

This 16-mark question has a full step-by-step worked solution and mark scheme. One marking point: Accurate zwitterion drawings at pH 1 and pH 5.9.

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