Chemistry 5070 · O Level · Separation and purification

Separation and purification — practice question

Using the apparatus shown, a student separates propanoic acid (b.p. $141\,^{\circ}\text{C}$) from butanoic acid (b.p. $164\,^{\circ}\text{C}$).
(a)[1]

Explain why the receiver flask has to be left open.

(b(i))[1]

What temperature is shown on the thermometer when the first drops of liquid reach the receiver flask?

(b(ii))[1]

What is the name of this liquid?

(b(iii))[1]

How can the student tell that all of this liquid has passed over?

(c)[1]

Suggest a safety item that the student should wear for this experiment.

Worked solution & mark scheme

This 5-mark question has a full step-by-step worked solution and mark scheme. One marking point: To stop pressure building up / to prevent explosion / to stop pressure increasing

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