Chemistry 5070 · O Level · Separation and purification

Separation and purification — practice question

A student uses the apparatus shown to separate hexane, $\text{C}_6\text{H}_{14}$, (b.p. $69^{\circ}\text{C}$) from heptane, $\text{C}_7\text{H}_{16}$, (b.p. $98^{\circ}\text{C}$).
(a)[2]

Identify two mistakes in the apparatus used by the student.

(b(i))[1]

Name apparatus A in the diagram.

(b(ii))[1]

What is apparatus A used for?

(b(iii))[1]

Name apparatus B in the diagram.

(b(iv))[1]

What is apparatus B used for?

(c(i))[1]

What is the thermometer reading when the first few drops of liquid appear, in C?

(c(ii))[1]

Name the liquid shown.

(d)[2]

Suggest a suitable method for heating the mixture and explain why you chose it.

Worked solution & mark scheme

This 10-mark question has a full step-by-step worked solution and mark scheme. One marking point: Thermometer/bulb too low / should be higher / must not touch beads / should be at entrance to condenser

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