Chemistry 5070 · O Level · Experimental design

Experimental design — practice question

Copper(II) sulfate crystals include water of crystallisation, which can be driven off by heating.
(a)[5]

You need to design an experiment to determine the percentage, by mass, of water in copper(II) sulfate crystals. Your plan should: • describe, or sketch, the apparatus that can be used to remove the water, • state all the weighings that ought to be taken, • explain how these can be used to calculate the percentage, by mass, of water.

(b)[3]

The formula for copper(II) sulfate crystals is $\text{CuSO}_4\cdot y\text{H}_2\text{O}$, where $y$ represents the number of moles of water of crystallisation in 1 mole of crystals. A student carries out an experiment and finds $y = 4$. The correct value of $y$ for her sample is $5$. Suggest an error in her experiment that would produce this difference. Explain how this error would cause the lower value of $y$ and suggest how the experiment could be improved so that the correct value of $y$ is obtained.

Worked solution & mark scheme

This 8-mark question has a full step-by-step worked solution and mark scheme. One marking point: Measure the crystals / record the mass before heating

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