Chemistry 9701 · AS & A Level · Chemistry of transition elements

Chemistry of transition elements — practice question

Complexes are produced when transition metal atoms or transition metal ions bond with ligands.
(a)[1]

Explain why transition elements are able to form complex ions.

(b(i))[2]

The $\text{Co}^{2+}$ ions make complex ion $G$. Each $G$ ion contains two $\text{Co}^{2+}$ ions, and each metal centre is octahedrally coordinated. One $\text{O}_2$ molecule is present in each $G$ ion and donates one pair of electrons to each $\text{Co}^{2+}$ ion, while one $\text{NH}_2^-$ ion does the same. The other ligands are $\text{NH}_3$ molecules. Deduce the formula of complex ion $G$. Include its overall charge.

(b(ii))[1]

The d-orbitals of the $\text{Co}^{2+}$ ions present in complex ion $G$ are split. State how many d-orbitals are at a higher energy level and how many are at a lower energy level in each $\text{Co}^{2+}$ ion.

(b(iii))[2]

The $\text{Co}^{2+}$ ions make a different complex ion, $M$. Each $M$ ion contains two $\text{Co}^{2+}$ ions, both of which are octahedrally coordinated, but the ligands differ from those in $G$. Explain why $G$ and $M$ have different colours.

(b)

The $Co^{2+}$ ions make complex ion G. Each G ion contains two Co$^{2+}$ ions, and each one is octahedrally coordinated. One O$_2$ molecule is present in each G ion and donates one pair of electrons to each Co$^{2+}$ ion, and one NH$_2^-$ ion donates one pair of electrons to each Co$^{2+}$ ion. The remaining ligands are NH$_3$ molecules.

(c)

Cadmium forms complex ion X, $\text{[Cd(NH}_3)_4\text{]}^{2+}$. When CN$^-$ ions are added to an aqueous solution of X, ligand exchange occurs and complex ion Y is produced. Y contains no NH$_3$ ligands and no H$_2$O ligands. Y is present at a much higher concentration in the mixture than X. The oxidation state and coordination number of cadmium stay the same in this reaction.

(c(i))[2]

Write an ionic equation for this reaction, using the formulae of the complex ions.

(c(ii))[1]

Cadmium forms complex ion Z with the same oxidation state and coordination number as in X. Every ligand in Z is Cl$^-$. When NaCl(aq) is added to a solution of X, only a very small amount of Z forms. Write the three cadmium complexes, X, Y and Z, in order of increasing stability constant, $K_{\text{stab}}$.

(d)

Ethanedioate ions, C$_2$O$_4^{2-}$, can form complexes with transition element ions. Their concentration can be determined by reacting them with acidified Cr$_2$O$_7^{2-}$ ions. The C$_2$O$_4^{2-}$ ions are protonated to form HOOCCOOH molecules, which are oxidised by Cr$_2$O$_7^{2-}$. The half-equations are shown: Cr$_2$O$_7^{2-} + 14\text{H}^+ + 6e^- \rightleftharpoons 2\text{Cr}^{3+} + 7\text{H}_2\text{O}$ and $2\text{CO}_2 + 2\text{H}^+ + 2e^- \rightleftharpoons \text{HOOCCOOH}$.

(d(i))[1]

Construct an equation for the reaction of acidified Cr$_2$O$_7^{2-}$ with HOOCCOOH.

(d(ii))[2]

A $25.0\text{ cm}^3$ portion of a Na$_2$C$_2$O$_4$ solution reacts exactly with $16.20\text{ cm}^3$ of $0.0500\text{ mol dm}^{-3}$ K$_2$Cr$_2$O$_7$(aq) after acidification. Calculate the concentration of the Na$_2$C$_2$O$_4$ solution.

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