Chemistry 9701 · AS & A Level · Chemistry of transition elements

Chemistry of transition elements — practice question

A transition element is a d-block element that forms one or more stable ions with partially filled d-orbitals.
(a)[1]

Among the 3d orbitals, two are the $3d_{xy}$ orbital and the $3d_{z^2}$ orbital. Sketch the shapes of these two orbitals.

(b(i))[4]

The $\text{Ni}^{2+}$ ion can form many different complexes. A solution containing the $[\text{Ni}(\text{H}_2\text{O})_6]^{2+}$ complex ion is green. When an excess of 1,2-diaminoethane, en, $\text{H}_2\text{NCH}_2\text{CH}_2\text{NH}_2$, is added, the solution turns blue. This happens because the $[\text{Ni}(en)_3]^{2+}$ complex ion is formed. Explain why the two solutions are coloured, and why the colours differ.

(b(ii))[1]

The $\text{[Ni(en)}_3]^{2+}$ complex can exist as a mixture of two stereoisomers. Complete the three-dimensional diagram so that it shows one stereoisomer. Each $en$ ligand may be represented by $\text{N-CH}_2\text{CH}_2\text{-N}$.

(b(iii))[1]

Name the geometry of the complex ion shown in (b)(ii) and the type of stereoisomerism displayed by $\text{[Ni(en)}_3]^{2+}$.

(c)[2]

Iron(II) carbonate, $\text{FeCO}_3$, and nickel(II) carbonate, $\text{NiCO}_3$, both decompose on heating. $\text{FeCO}_3$ breaks down at a lower temperature than $\text{NiCO}_3$. Suggest one possible explanation for this difference. Explain your answer.

(d(i))[1]

Describe the colour change observed in the conical flask at the end-point of this titration. The colour changes from ................ to ................ .

(d(ii))[2]

Calculate the percentage by mass of iron present in $A$. $[A_r: \text{Fe}, 55.8]$.

Worked solution & mark scheme

This 12-mark question has a full step-by-step worked solution and mark scheme. One marking point: Correct labels for $3d_{xy}$ and $3d_{z^2}$

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