Chemistry 9701 · AS & A Level · Chemistry of transition elements

Chemistry of transition elements — practice question

(a)[2]

Write out the electronic configurations for these ions. $\text{Cr}^{3+}: 1s^2 2s^2 2p^6 \ldots$ $\text{Mn}^{2+}: 1s^2 2s^2 2p^6 \ldots$

(b(i))

$\text{KMnO}_4$ and $\text{K}_2\text{Cr}_2\text{O}_7$ both act as oxidising agents, generally in acidic solution. Use the Data Booklet to explain why their oxidising power becomes greater as the $[\text{H}^+(aq)]$ in the solution increases.

(b(ii))[4]

What colour changes would you see when each of these oxidising agents is fully reduced? $\text{KMnO}_4$: from \ldots\ldots\ldots\ldots\ldots\ldots to \ldots\ldots\ldots\ldots\ldots\ldots $\text{K}_2\text{Cr}_2\text{O}_7$: from \ldots\ldots\ldots\ldots\ldots\ldots to \ldots\ldots\ldots\ldots\ldots\ldots

(c(i))

Manganese(IV) oxide, $\text{MnO}_2$, is a dark brown solid that does not dissolve in water or dilute acids. However, bubbling a stream of $\text{SO}_2(g)$ through a suspension of $\text{MnO}_2$ in water causes it to dissolve and form a colourless solution. Use the Data Booklet to propose an equation for this reaction, and explain how the oxidation states of manganese and sulfur change during the process.

(c(ii))[4]

The pH of the $\text{MnO}_2$ suspension is lowered. Explain what effect, if any, this would have on the extent of this reaction.

(d(i))

The principal manganese ore, pyrolusite, is mostly $\text{MnO}_2$. A $\text{SnCl}_2$ solution can be used, by the method given, to determine the percentage of $\text{MnO}_2$ in a pyrolusite sample. Use the Data Booklet to form an equation for the reaction between $\text{MnO}_2$ and $\text{Sn}^{2+}(aq)$ ions in acidic solution.

(d(ii))[6]

Calculate the percentage of $\text{MnO}_2$ in this pyrolusite sample by carrying out the following steps: • number of moles of $\text{MnO}_4^-$ used in the titration • number of moles of $\text{Sn}^{2+}$ this $\text{MnO}_4^-$ reacted with • number of moles of $\text{Sn}^{2+}$ that reacted with the $0.100\,\text{g}$ sample of pyrolusite • number of moles of $\text{MnO}_2$ in $0.100\,\text{g}$ pyrolusite. Use your equation in (i) • mass of $\text{MnO}_2$ in $0.100\,\text{g}$ pyrolusite • percentage of $\text{MnO}_2$ in pyrolusite

Worked solution & mark scheme

This 16-mark question has a full step-by-step worked solution and mark scheme. One marking point: $\text{Cr}^{3+}: 1s^2 2s^2 2p^6 3s^2 3p^6 3d^3$

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