Chemistry 9701 · AS & A Level · Carboxylic acids and derivatives

Carboxylic acids and derivatives — practice question

A structural formula for glycolic acid is displayed.
(a)[4]

Fill in the table to show what you would observe when an aqueous solution of glycolic acid is added separately to each reagent. If a reaction happens, give the functional group of glycolic acid that causes it.

(b(i))[1]

Draw a structure for $\text{X}$.

(b)

Two routes for making glycolic acid are shown: sequence A: $\text{HCHO} \xrightarrow[\text{reaction 1}]{\text{HCN and NaCN}} X \xrightarrow[\text{reaction 2}]{} \text{CH}_2(\text{OH})\text{CO}_2\text{H}$; sequence B: $\text{CH}_3\text{CO}_2\text{H} \xrightarrow[\text{reaction 3}]{\text{Br}_2} \text{CH}_2\text{BrCO}_2\text{H} \xrightarrow[\text{reaction 4}]{} \text{CH}_2(\text{OH})\text{CO}_2\text{H}$.

(b(ii))[1]

Name the reagent for reaction 2.

(b(iii))[1]

Name the mechanism of reaction 3.

(b(iv))[1]

Suggest the essential condition for reaction 3.

(b(v))[2]

Reaction 4 proceeds by an $S_N2$ mechanism. Complete the mechanism diagram for reaction 4. Include all relevant charges, partial charges, curly arrows and lone pairs.

(c)

Glycolic acid can also be prepared by reacting glyoxylic acid with $\text{NaBH}_4$.

(c(i))[1]

State the role of $\text{NaBH}_4$ in this reaction.

(c(ii))[2]

Write an equation for this reaction using molecular formulae. Use $[\text{H}]$ to represent $\text{NaBH}_4$.

(d)

When glycolic acid is heated with a sulfuric acid catalyst, a new compound, $Y$, $\text{C}_4\text{H}_4\text{O}_4$, is produced. The equation for the reaction is given: $2\text{CH}_2(\text{OH})\text{CO}_2\text{H} \rightarrow \text{C}_4\text{H}_4\text{O}_4 + 2\text{H}_2\text{O}$.

(d(i))[2]

The infra-red spectrum of $Y$ is shown. State how this spectrum is different from an infra-red spectrum of glycolic acid. Explain your answer with particular reference to the peaks in the range $1500$-$4000\ \text{cm}^{-1}$.

(d(ii))[2]

Suggest a structure for $Y$.

Worked solution & mark scheme

This 17-mark question has a full step-by-step worked solution and mark scheme. One marking point: Fizzing with $\mathrm{Na_2CO_3}$

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