Chemistry 9701 · AS & A Level · Analytical techniques

Analytical techniques — practice question

Acidified potassium dichromate(VI) is able to oxidise ethanedioic acid, $\text{H}_2\text{C}_2\text{O}_4$. The two relevant half-equations are given below: $\text{Cr}_2\text{O}_7^{2-} + 14\text{H}^+ + 6e^- \rightarrow 2\text{Cr}^{3+} + 7\text{H}_2\text{O}$ $\text{H}_2\text{C}_2\text{O}_4 \rightarrow 2\text{CO}_2 + 2\text{H}^+ + 2e^-$
(a)[2]

State the complete equation for the reaction of acidified dichromate(VI) ions with ethanedioic acid.

(b(i))[1]

Calculate the amount, in moles, of dichromate(VI) ions that reacted with the ethanedioic acid sample.

(b(ii))[1]

Calculate the amount, in moles, of ethanedioic acid in the sample.

(b(iii))[1]

Calculate the relative molecular mass, $M_r$, of the hydrated ethanedioic acid.

(b(iv))[1]

Calculate the value of $x$ in $\text{H}_2\text{C}_2\text{O}_4 \cdot x\text{H}_2\text{O}$.

Worked solution & mark scheme

This 6-mark question has a full step-by-step worked solution and mark scheme. One marking point: Correctly balanced equation $Cr_2O_7^{2-} + 8H^+ + 3H_2C_2O_4 \rightarrow 2Cr^{3+} + 6CO_2 + 7H_2O$

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